HuagongsheHuagongshe Chemistry Print Report · For research reference only
Alpha-Methylstyrene → HCID 5152757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Alpha-Methylstyrene | HCID 7407 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | HCID 5152757 | HCID 5152757 | — |
Reaction Steps
100 g of N-bromosuccinimide are added to the mixture of 250 ml of α-methylstyrene and 40 ml of carbon tetrachloride. The resulting mixture is heated to reflux for 5 min. and cooled in an ice-water bath. Filtration and concentration give the desired compound, 1-bromo-2-phenylpropene, and an isomer thereof (65:35).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06673850B1 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-7593fdc00e4340b0b54db76a6d7a837c |
| Source note | uspto-grants-2004_01 |