HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Nitrophenol → 1-(3-bromopropoxy)-2-nitrobenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Nitrophenol | HCID 6947 | — |
| Reactant | 1,3-Dibromopropane | HCID 8001 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 1-(3-bromopropoxy)-2-nitrobenzene | HCID 7172300 | — |
Reaction Steps
In analogy to the procedure described in example 5) (a) 2-nitrophenol was treated with sodium carbonate followed by 1,3-dibromo-propane in N,N-dimethylformamide to yield the 1-(3-bromo-propoxy)-2-nitro-benzene as slightly green solid; MS: 259, 261 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06673931B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-ec2d9d38d4ff452ba8243f55bc471a92 |
| Source note | uspto-grants-2004_01 |