2,4,6-Trimethylpyridine → HCID 23449633, compound

Participants

Reaction Steps

To a solution of the compound prepared in example 1 (2.52 g) in dimethylformamide (30 ml) were added 2,4,6-collidine (3.96 ml), mesyl chloride (929 μl) and lithium chloride (593 mg). The mixture was stirred for 2 hours at room temperature. The reaction mixture was poured into water and the precipitate was collected by filtration. The precipitate was washed with water, methanol and ether to give the title compound (2.50 g) having the following physical data.

Provenance & Evidence