HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorophenol → HCID 9021527, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorophenol | HCID 7245 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 9317226 | HCID 9317226 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 9021527 | HCID 9021527 | — |
Reaction Steps
To a solution of 9 (0.194g, 0.6mmol) in 4ml acetone was added 2-chlorophenol (0.092g, 0.72mmol) and potassium carbonate (0.3g, 2.2mmol). The solution was heated to reflux and stirred for 48h. The solution was filtered to remove potassium carbonate, concentrated en vacuo, and purified by Prep TLC (10:1 DCM:MeOH) to yield compound 11. Mass spectrum (M+1)=416.32
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06677343B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-9ea8d15f6761414b970fe588f2180a5c |
| Source note | uspto-grants-2004_01 |