Benzenesulfonyl chloride → HCID 9978881, compound

Participants

Reaction Steps

Using the general method of Example 232, 1-(4-aminobutyl)-2-methyl-1H-imidazo[4,5-c]quinolin-4-amine (0.50 g, 1.9 mmol) was reacted with benzenesulfonyl chloride (0.24 mL, 1.9 mmol) to provide 0.38 g of N-[4-(4-amino-2-methyl-1H-imidazo[4,5-c]quinolin-1-yl)butyl]benzenesulfonamide as brown granules, m.p. 215.4-216.0° C. Analysis: Calculated for C21H23N5O2S: %C, 61.59; %H, 5.66; %N, 17.10; Found %C, 61.24; %H, 5.65; %N, 16.95.

Provenance & Evidence