HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 22344417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | 4-(2-Hexyl-1H-imidazo[4,5-c]quinolin-1-yl)butan-1-amine | HCID 22344437 | — |
| Product | HCID 22344417 | HCID 22344417 | 92.2% |
Reaction Steps
Using the general method of Example 232, 4-(2-hexyl-1H-imidazo[4,5-c]quinolin-1-yl)butan-1-amine (1.00 g, 3.1 mmol) was reacted with methanesulfonyl choride (0.48 mL, 6.2 mmol) to provide 1.15 g of N-[4-(2-hexyl-1H-imidazo[4,5-c]quinolin-1-yl)butyl]methanesulfonamide as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06677349B1 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-3ac896da08814baeb211503750eaa0c0 |
| Source note | uspto-grants-2004_01 |