Benzenesulfonyl chloride → HCID 11743917, compound

Participants

Reaction Steps

Using the general method of Example 242, 1-(3-aminopropyl)-2-(2-methoxyethyl)-1H-imidazo[4,5-c]quinolin-4-amine (1.53 g, 5.11 mmol) was reacted with benzenesulfonyl chloride (993 mg, 5.62 mmol) to provide 1.37 g of N-{3-[4-amino-2-(2-methoxyethyl)-1H-imidazo[4,5-c]quinolin-1-yl]propyl}benzenesulfonamide as a white powder, m.p. 149-151° C. Analysis: Calculated for C22H25N5O3S: %C, 60.12; %H, 5.73; %N, 15.93; Found: %C, 60.40; %H, 5.82; %N, 15.85.

Provenance & Evidence