Benzenesulfonyl chloride → HCID 10389776, compound

Participants

Reaction Steps

Using the general method of Example 232, 1-(4-aminobutyl)-2-pentyl-1H-imidazo[4,5-c]quinolin-4-amine (1.00 g, 3.1 mmol) was reacted with benzenesulfonyl chloride (0.51 mL, 4.0 mmol) to provide 0.35 g of N-[4-(4-amino-2-pentyl-1H-imidazo[4,5-c]quinolin-1-yl)butyl]benzenesulfonamide as a yellow crystalline solid. Analysis: Calculated for C25H31N5O2S.0.5 H2O: %C, 63.27; %H, 6.80; %N, 14.76; Found: %C, 62.99; %H, 6.61; %N, 14.42.

Provenance & Evidence