Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | HCID 69827849 | HCID 69827849 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86588181 | HCID 86588181 | — |
Reaction Steps
A mixture of 1-[(3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyltetrahydrofuro[3,4-d][1,3]dioxol-4-yl]pent-1-yn-3-one (550 mg) and hydroxylamine (50% solution in water) (0.2 ml) in ethanol (10 ml) was stirred overnight at 22° C. The mixture was concentrated in vacuo to afford the title compound as a yellow oil (554 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06677316B2 |
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| Source dataset | uspto-grants-2004_01 |
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| ORD ID | ord-72841c04c84a47a7ba81c4b1d4cbf916 |
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| Source note | uspto-grants-2004_01 |
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