4-Cyanobenzoyl chloride → HCID 10547191, compound

HRID 1839458Notes

Reaction equation

HRID 1839458 reaction equation
[CH3:1][O:2][C:3]1[CH:18]=[CH:17][C:6]([C:7]([NH:9][C:10]2[C:11]([NH2:16])=[CH:12][CH:13]=[CH:14][CH:15]=2)=[O:8])=[CH:5][CH:4]=1.[C:19]([C:21]1[CH:29]=[CH:28][C:24]([C:25](Cl)=[O:26])=[CH:23][CH:22]=1)#[N:20]>>[C:19]([C:21]1[CH:29]=[CH:28][C:24]([C:25]([NH:16][C:11]2[C:10]([NH:9][C:7](=[O:8])[C:6]3[CH:5]=[CH:4][C:3]([O:2][CH3:1])=[CH:18][CH:17]=3)=[CH:15][CH:14]=[CH:13][CH:12]=2)=[O:26])=[CH:23][CH:22]=1)#[N:20]

Participants

3

Reactant 2

HCID 801724-Cyanobenzoyl chlorideHCID 785232N-(2-Aminophenyl)-4-methoxybenzamide

Product 1

HCID 10547191HCID 10547191, compound

Procedure

Using a procedure similar to Example 1B except starting with N1-(4-methoxybenzoyl)-1,2-benzenediamine and 4-cyanobenzoyl chloride, the title compound was obtained as a solid (59%); MS(FD): 371.0.

Sources & evidence

ORD record
ord-56a4d328defc47bca2159590963192ea
Source dataset
uspto-grants-2004_01
Patent number
US06677369B2

Reaction notes

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