4-Ethoxybenzoyl Chloride → HCID 11794488, compound

Participants

Reaction Steps

Using a procedure similar to 1B except starting with N1-(3-cyanobenzoyl)-1,2-benzenediamine, 4-ethoxybenzoyl chloride and triethylamine as base, the title compound was obtained as a white solid (39%); mp: 168-9° C.; IR(KBr): 1645, 1672, 2231, 3377 cm−1; MS(FD): 385(M+). NMR(300 MHz, DMSO-d6): δ1.31 (t, 3 H); 4.07 (quartet, 2 H); 7.03 (d, 2 H); 7.30 (m, 2 H); 7.60 (m, 2 H); 7.72 (t, 1 H); 7.91 (d, 2 H); 8.04 (d, 2 H); 8.21 (d, 1 H); 8.35 (s, 1 H)

Provenance & Evidence