1-Bromopropane → HCID 15518502, compound

HRID 1840264Notes

Reaction equation

HRID 1840264 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=3)=[N:13][NH:12][C:11](=[O:23])[C:10]=2[C:24]#[N:25])=[CH:5][CH:4]=1.Br[CH2:27][CH2:28][CH3:29]>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=3)=[N:13][N:12]([CH2:27][CH2:28][CH3:29])[C:11](=[O:23])[C:10]=2[C:24]#[N:25])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 78401-BromopropaneHCID 126885835,6-bis(4-methoxyphenyl)-4-cyano-2H-pyridazin-3-one

Product 1

HCID 15518502HCID 15518502, compoundYield 72.6%

Procedure

Using 5,6-bis(4-methoxyphenyl)-4-cyano-2H-pyridazin-3-one and 1-bromopropane as starting materials, the procedures of Example 1 were repeated likewise, whereby the title compound was obtained in a yield of 72.6%.

Sources & evidence

ORD record
ord-e664829c67de442c85956e980ac21df6
Source dataset
uspto-grants-2004_01
Patent number
US06680316B1

Reaction notes

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