Aniline → HCID 23447729, compound

HRID 1840271Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=3)=[N:13][N:12]([CH2:23][CH:24]([CH3:26])[CH3:25])[C:11](=[O:27])[C:10]=2[C:28](O)=[O:29])=[CH:5][CH:4]=1.[NH2:31][C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=3)=[N:13][N:12]([CH2:23][CH:24]([CH3:25])[CH3:26])[C:11](=[O:27])[C:10]=2[C:28](=[O:29])[NH:31][C:32]2[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=2)=[CH:5][CH:4]=1

Participants

Reactant 2

HCID 6115Aniline

HCID 15518516HCID 15518516, compound

Product 1

HCID 23447729HCID 23447729, compoundYield 89%

Procedure

Using 5,6-bis(4-methoxyphenyl)-4-carboxy-2-isobutyl-2H-pyridazin-3-one and aniline as starting materials, the procedures of Example 22 were repeated likewise, whereby the title compound was obtained in a yield of 89.0%.

Sources & evidence

ORD record: ord-a16d75c4235448d68ebe6a94c4da8646
Source dataset: uspto-grants-2004_01
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06680316B1

Reaction notes

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