Benzylamine → HCID 12114198, compound
Reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[C:14]([C:15]3[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=3)=[N:13][N:12]([CH2:23][CH:24]3[CH2:26][CH2:25]3)[C:11](=[O:27])[C:10]=2[C:28](O)=[O:29])=[CH:5][CH:4]=1.[CH2:31]([NH2:38])[C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1>>[CH2:31]([NH:38][C:28]([C:10]1[C:11](=[O:27])[N:12]([CH2:23][CH:24]2[CH2:26][CH2:25]2)[N:13]=[C:14]([C:15]2[CH:20]=[CH:19][C:18]([O:21][CH3:22])=[CH:17][CH:16]=2)[C:9]=1[C:6]1[CH:7]=[CH:8][C:3]([O:2][CH3:1])=[CH:4][CH:5]=1)=[O:29])[C:32]1[CH:37]=[CH:36][CH:35]=[CH:34][CH:33]=1Participants
3
Procedure
Using 5,6-bis(4-methoxyphenyl)-4-carboxy-2-cyclopropylmethyl-2H-pyridazin-3-one and benzylamine as starting materials, the procedures of Example 22 were repeated likewise, whereby the title compound was obtained quantitatively.
Sources & evidence
- ORD record
- ord-85474f73f84d47238b756f0029855ce6
- Source dataset
- uspto-grants-2004_01
- Patent number
- US06680316B1
Reaction notes
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