HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylphenyl isothiocyanate → HCID 23447739, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylphenyl isothiocyanate | HCID 69195 | — |
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | N,N-Dimethyl-3-amino-6-chloro-2-hydroxybenzenesulfonamide | HCID 23447758 | — |
| Product | HCID 23447739 | HCID 23447739 | 70% |
Reaction Steps
Following the general procedure for thiourea formation outlined in example 12, N,N-dimethyl-3-amino-6chloro-2-hydroxybenzenesulfonamide (500 mg, 2 mmol) and 2-methylphenylisothiocyanate (298.4 mg, 2 mmol) were coupled to form the desired thiourea (557 mg, 70%). EI-MS m/z 400.0 (M30 ).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06680317B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-1850492e0dd04e55b7b2120277932e12 |
| Source note | uspto-grants-2004_01 |