HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiourea → HCID 23447736, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiourea | HCID 2723790 | — |
| Reactant | N,N-Dimethyl-3-amino-6-chloro-2-hydroxybenzenesulfonamide | HCID 23447758 | — |
| Reactant | HCID 23447830 | HCID 23447830 | — |
| Product | HCID 23447736 | HCID 23447736 | 71.1% |
Reaction Steps
Following the general procedure for thiourea formation outlined in example 12, N,N-dimethyl-3-amino-6-chloro-2-hydroxybenzenesulfonamide (500 mg, 2.0 mmol) and 2chloro-3-fluorophenylisothiocyanate (374 mg, 2.0 mmol) were coupled to form the desired thiourea (623 mg, 71%). LC-MS m/z 438.2 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06680317B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-b8a8042ed58244f0b967a8a6e4336b86 |
| Source note | uspto-grants-2004_01 |