HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Methylethylenediamine → 3-Methoxy-6-(2-methylamino-ethylamino)-5,9-diaza-benzo[c]fluoren-7-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Methylethylenediamine | HCID 8014 | — |
| Reactant | 6-(2-Dimethylamino-ethylamino)-3-methoxy-5,10-diaza-benzo[c]-fluoren-7-one | HCID 9946287 | — |
| Product | 3-Methoxy-6-(2-methylamino-ethylamino)-5,9-diaza-benzo[c]fluoren-7-one | HCID 10268573 | — |
Reaction Steps
This compound was prepared from the compound of Example 1c-2 and N-methylethylenediamine. The desired product was obtained as a red solid. EI−MS: m/z 334 (M+); 1H-NMR (CDCl3): δ2.51 (3H, s), 2.94 (2H, t, J=6 Hz), 3.82 (2H, d, J=6 Hz), 3.97 (3H, s), 6.98 (1H, dd, J=9 Hz, 2.5 Hz), 7.10 (1H, d, J=2.5 Hz), 7.88 (1H, dd, J=5 Hz, 1 Hz), 8.05 (1H, d, J=9 Hz), 8.84 (1H, d, 5 Hz), 8.87 (1H, d, J=1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06680326B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-ad6996fd21fa4c489caa1ef84ee06303 |
| Source note | uspto-grants-2004_01 |