HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Iodophenol → 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Iodophenol | HCID 10784 | — |
| Reactant | Phenylboronic acid pinacol ester | HCID 570673 | — |
| Product | 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)phenol | HCID 2734623 | — |
Reaction Steps
The above reaction procedure used for 2-iodophenol was followed. The reaction was faster, being complete before the first sample for gc analysis was withdrawn after 1 h 50 min reaction time. The amount of phenylboronic acid pinacol ester was higher than in the 2-iodophenol reaction (around 7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06680401B1 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-226c68600d184201b4f41afaab0d1b8b |
| Source note | uspto-grants-2004_01 |