HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, (2-iodoethyl)- → 6-Acetyl-4,4-dimethyl-1-(2-phenylethyl)-3,4-dihydroquinolin-2(1H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, (2-iodoethyl)- | HCID 28503 | — |
| Reactant | 2(1H)-Quinolinone, 6-acetyl-1-hexyl-3,4-dihydro-4,4-dimethyl- | HCID 12135416 | — |
| Product | 6-Acetyl-4,4-dimethyl-1-(2-phenylethyl)-3,4-dihydroquinolin-2(1H)-one | HCID 69890883 | 34% |
Reaction Steps
Following a procedure similar to that used for the preparation of Intermediate 6a but using (2-iodo-ethyl)benzene as the alkylating reagent the title compounds was obtained as a colorless oil (34% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06683092B1 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-f3dedc273e0c4c39bd421954b290e39d |
| Source note | uspto-grants-2004_01 |