1199-20-8 → HCID 69684627, compound

HRID 1840894Notes

Reaction equation

HRID 1840894 reaction equation
Cl.Cl.[N:3]12[CH2:10][CH2:9][CH:6]([CH2:7][CH2:8]1)[C@@H:5]([NH2:11])[CH2:4]2.[CH3:12]/[C:13](/[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)=[CH:14]\[C:15](O)=[O:16]>>[N:3]12[CH2:10][CH2:9][CH:6]([CH2:7][CH2:8]1)[C@@H:5]([NH:11][C:15](=[O:16])/[CH:14]=[C:13](\[CH3:12])/[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)[CH2:4]2

Participants

3

Reactant 2

HCID 53546611199-20-8HCID 12494972(R)-(+)-3-Aminoquinuclidine Dihydrochloride

Product 1

HCID 69684627HCID 69684627, compound

Procedure

Prepared as a free base by a method analogous to that described in Example 1 from (R)-1-azabicyclo[2.2.2]oct-3-ylamine dihydrochloride and E-3-methyl-3-phenylpropenoic acid, giving a light tan solid; MS (ES+) 271 (MH+).

Workup

  1. customPrepared as a free base by a method analogous to
  2. customgiving a light tan solid

Sources & evidence

ORD record
ord-8984e2a71d974074bc4a07f4190532d4
Source dataset
uspto-grants-2004_01
Patent number
US06683090B1

Reaction notes

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