Piperonylamine → HCID 11380435, compound

HRID 1840952Notes

Reaction equation

HRID 1840952 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][CH:8]=[CH:7]2.Cl.O.[NH:13]1[CH2:18][CH2:17][C:16](=O)[CH2:15][CH2:14]1>>[Br:1][C:2]1[CH:3]=[CH:4][CH:5]=[C:6]2[C:10]=1[NH:9][CH:8]=[C:7]2[CH:16]1[CH2:17][CH2:18][NH:13][CH2:14][CH2:15]1

Participants

3

Reactant 2

HCID 2723901PiperonylamineHCID 27570207-Bromoindole

Product 1

HCID 11380435HCID 11380435, compound

Procedure

This compound was prepared following the procedure described in Example 1 (parts A and B) starting with 0.95 g (4.8 mmol) of 7-bromoindol and 1.89 g (12.3 mmol) of 4-piperidone monohydrate hydrochloride. After the usual work-up 1.1 g (89% of yield) of the desired product were obtained.

Workup

  1. customThis compound was prepared

Sources & evidence

ORD record
ord-9a6614580d96446899fd8e45bfdd288c
Source dataset
uspto-grants-2004_01
Patent number
US06683096B2

Reaction notes

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