HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminumhydride → HCID 23445131, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminumhydride | HCID 21225700 | — |
| Reactant | HCID 69042755 | HCID 69042755 | — |
| Product | HCID 23445131 | HCID 23445131 | — |
Reaction Steps
Following the general method described in example 388, 1-quinolin-6-yl-1H-imidazole-4-carboxylic acid ethyl ester was reacted with diisobutylaluminum hydride. After hydrolytic workup and chromatography the title compound was obtained as a light brown crystalline solid. Mp. 183-187° C. (AcOEt/hexane), MS: m/e=226 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06683097B2 |
| Source dataset | uspto-grants-2004_01 |
| ORD ID | ord-ec589a836a284373afbee8976b697a1b |
| Source note | uspto-grants-2004_01 |