Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Hydroxy-5-methylacetophenone → (e)-3-(2-Bromo-3,4-dimethoxyphenyl)-1-(2-hydroxy-5-methylphenyl)-2-propen-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Hydroxy-5-methylacetophenone | HCID 15068 | — |
| 반응물 | 2-Bromo-3,4-dimethoxybenzaldehyde | HCID 618538 | — |
| 생성물 | (e)-3-(2-Bromo-3,4-dimethoxyphenyl)-1-(2-hydroxy-5-methylphenyl)-2-propen-1-one | HCID 23444786 | 65.1% |
반응 단계
2-Hydroxy-5-methylacetophenone (85 mg, 0.57 mmol) and 2-bromo-3,4-dimethoxybenzaldehyde (166 mg, 0.68 mmol) were reacted according to the same procedure as Preparation 1 to give 140 mg (Yield 54.6%) of the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06683095B2 |
| 출처 데이터셋 | uspto-grants-2004_01 |
| ORD ID | ord-aee211e4d1034779ae014ec73b20b796 |
| 출처 메모 | uspto-grants-2004_01 |