Phenyl N-(2-methoxyquinoxalin-3-yl)carbamate → 1-[(2-Methoxyquinoxalin-3-yl)aminocarbonyl]-4-(3,5-dinitrophenyl)piperazine

HRID 1841480Notes

Reaction equation

HRID 1841480 reaction equation
[CH3:1][O:2][C:3]1[C:12]([NH:13][C:14](=[O:22])OC2C=CC=CC=2)=[N:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=1.[N+:23]([C:26]1[CH:27]=[C:28]([N:35]2[CH2:40][CH2:39][NH:38][CH2:37][CH2:36]2)[CH:29]=[C:30]([N+:32]([O-:34])=[O:33])[CH:31]=1)([O-:25])=[O:24]>>[CH3:1][O:2][C:3]1[C:12]([NH:13][C:14]([N:38]2[CH2:39][CH2:40][N:35]([C:28]3[CH:29]=[C:30]([N+:32]([O-:34])=[O:33])[CH:31]=[C:26]([N+:23]([O-:25])=[O:24])[CH:27]=3)[CH2:36][CH2:37]2)=[O:22])=[N:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=1

Participants

3

Reactant 2

HCID 23446261Phenyl N-(2-methoxyquinoxalin-3-yl)carbamateHCID 234463481-(3,5-Dinitrophenyl)piperazine

Product 1

HCID 234462621-[(2-Methoxyquinoxalin-3-yl)aminocarbonyl]-4-(3,5-dinitrophenyl)piperazineYield 54.5%

Procedure

Phenyl N-(2-methoxyquinoxalin-3-yl)carbamate and 1-(3,5-dinitrophenyl)piperazine were reacted by the same way with the example 36 to obtain the titled compound.

Sources & evidence

ORD record
ord-0dc28bc12a4a4a2f8b1428417175856b
Source dataset
uspto-grants-2004_01
Patent number
US06683184B2

Reaction notes

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