1-(3-Bromophenyl)piperazine → HCID 86588091, compound

HRID 1841490Notes

Reaction equation

HRID 1841490 reaction equation
[CH3:1][O:2][C:3]1[C:12]([NH:13][C:14](=[S:22])OC2C=CC=CC=2)=[N:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=1.[Br:23][C:24]1[CH:25]=[C:26]([N:30]2[CH2:35][CH2:34][NH:33][CH2:32][CH2:31]2)[CH:27]=[CH:28][CH:29]=1>>[CH3:1][O:2][C:3]1[C:12]([NH:13][C:14]([N:33]2[CH2:32][CH2:31][N:30]([C:26]3[CH:27]=[CH:28][CH:29]=[C:24]([Br:23])[CH:25]=3)[CH2:35][CH2:34]2)=[S:22])=[N:11][C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=1

Participants

3

Reactant 2

HCID 27571541-(3-Bromophenyl)piperazineHCID 53676590Phenyl N-(2-methoxyquinoxalin-3-yl)thiocarbamate

Product 1

HCID 86588091HCID 86588091, compoundYield 57.5%

Procedure

Phenyl N-(2-methoxyquinoxalin-3-yl)thiocarbamate and 1-(3-bromophenyl)piperazine were reacted by the same way with the example 63 to obtain the titled compound.

Sources & evidence

ORD record
ord-f92113a084374474b3a21377ba97cd12
Source dataset
uspto-grants-2004_01
Patent number
US06683184B2

Reaction notes

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