1-(2-(Methylthio)phenyl)piperazine → HCID 23446155, compound

HRID 1841503Notes

Reaction equation

HRID 1841503 reaction equation
[CH2:1]([O:3][C:4]1[C:13]([NH:14][C:15](=[O:23])OC2C=CC=CC=2)=[N:12][C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]=1)[CH3:2].[CH3:24][S:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][C:27]=1[N:32]1[CH2:37][CH2:36][NH:35][CH2:34][CH2:33]1>>[CH2:1]([O:3][C:4]1[C:13]([NH:14][C:15]([N:35]2[CH2:34][CH2:33][N:32]([C:27]3[CH:28]=[CH:29][CH:30]=[CH:31][C:26]=3[S:25][CH3:24])[CH2:37][CH2:36]2)=[O:23])=[N:12][C:11]2[C:6](=[CH:7][CH:8]=[CH:9][CH:10]=2)[N:5]=1)[CH3:2]

Participants

3

Reactant 2

HCID 27368951-(2-(Methylthio)phenyl)piperazineHCID 23446273Phenyl N-(2-ethoxyquinoxalin-3-yl)carbamate

Product 1

HCID 23446155HCID 23446155, compoundYield 71.4%

Procedure

Phenyl N-(2-ethoxyquinoxalin-3-yl)carbamate and 1-(2-methylthiophenyl)piperazine were reacted by the same way with the example 36 to obtain the titled compound.

Sources & evidence

ORD record
ord-437cce787e124ffd814c1e79e2b818a1
Source dataset
uspto-grants-2004_01
Patent number
US06683184B2

Reaction notes

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