Benzoyl chloride → HCID 56942374, compound

Participants

Reaction Conditions

Reaction Steps

In a flask, dichloromethane (0.023mL) was added to benzoyl chloride. The reaction was cooled to 0° C., and a solution of N-(3-(pyridin-4-yl)-1H-indazol-5-yl)piperidine-3-carboxamide (0.014 g, 0.044 mmol) in dichloromethane (0.020 mL) was dropwise added to the benzoyl chloride solution. The reaction stirred for 6 hrs from 0° C. to room temperature. The reaction was quenched with water (1 mL) and extracted with dichloromethane (3×1 mL). The extracts were combined and dried with sodium sulfate. The crude product was purified using prep LC/MS. LC-MS: 426.1 [M+H]. LC/MS RT=2.998 min.

Provenance & Evidence