HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Acetylphenylboronic acid → N-[5-(3-acetylphenyl)-2,3-dihydro-1H-inden-2-yl]-2-propanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Acetylphenylboronic acid | HCID 2734310 | — |
| Reactant | N-(5-iodo-2,3-dihydro-1H-inden-2-yl)-2-propanesulfonamide | HCID 46899809 | — |
| Product | N-[5-(3-acetylphenyl)-2,3-dihydro-1H-inden-2-yl]-2-propanesulfonamide | HCID 11689005 | — |
Reaction Steps
The title compound was prepared from Intermediate 2 and (3-acetylphenyl)boronic acid (Sigma Aldrich Company Ltd.) using the method of Example 1; mass spectrum (API+): Found 358 (MH+), C20H23NO3S requires 357; 1H-NMR (400 MHz, CDCl3): 1.42 (6H, d, J=7 Hz), 2.66 (3H, s), 2.99 (2H, m), 3.20 (1H, m), 3.35 (2H, m), 4.29 (2H, m), 7.32 (1H, m), 7.46 (2H, m), 7.56 (1H, m), 7.76 (1H, m), 7.92 (1H, m), 8.14 (1H, m).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07741351B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-88d727a6626a46cbb465620735f1087c |
| Source note | uspto-grants-2010_06 |