HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 1122381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Benzylpiperazine | HCID 75994 | — |
| Reactant | Methoxyacetyl chloride | HCID 96623 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 1122381 | HCID 1122381 | — |
Reaction Steps
Amine preparation: a mixture of benzylpiperazine, methoxyacetyl chloride and triethylamine was stirred in DCM for 2 h to yield 1-(4-benzyl-piperazin-1-yl)-2-methoxy-ethanone following standard work up.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946217B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-de297241fbd946deb490093ef5da5d27 |
| Source note | uspto-grants-2015_02 |