2-Chloro-5-nitrophenol → HCID 50917623, compound

HRID 1842360Notes

Reaction equation

HRID 1842360 reaction equation
[OH:1][CH:2]1[CH2:7][CH2:6][N:5]([C:8](=[O:19])[CH2:9][NH:10][C:11]2[C:12](=[O:18])[N:13]([CH3:17])[N:14]=[CH:15][CH:16]=2)[CH2:4][CH2:3]1.[Cl:20][C:21]1[CH:26]=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][C:22]=1O>>[Cl:20][C:21]1[CH:26]=[CH:25][C:24]([N+:27]([O-:29])=[O:28])=[CH:23][C:22]=1[O:1][CH:2]1[CH2:3][CH2:4][N:5]([C:8](=[O:19])[CH2:9][NH:10][C:11]2[C:12](=[O:18])[N:13]([CH3:17])[N:14]=[CH:15][CH:16]=2)[CH2:6][CH2:7]1

Participants

3

Reactant 2

HCID 692642-Chloro-5-nitrophenolHCID 66957754HCID 66957754, compound

Product 1

HCID 50917623HCID 50917623, compoundYield 7%

Procedure

Compound 9 is prepared from intermediate 5b and from 2-chloro-5-nitro-phenol following synthesis method 3 (yield: 7%).

Sources & evidence

ORD record
ord-26ac985148834aea9b98935a687f78a3
Source dataset
uspto-grants-2015_02
Patent number
US08946225B2

Reaction notes

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