2-Nitrophenol → HCID 66957741, compound

HRID 1842362Notes

Reaction equation

HRID 1842362 reaction equation
[OH:1][CH:2]1[CH2:7][CH2:6][N:5]([C:8](=[O:19])[CH2:9][NH:10][C:11]2[C:12](=[O:18])[N:13]([CH3:17])[N:14]=[CH:15][CH:16]=2)[CH2:4][CH2:3]1.[N+:20]([C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][C:24]=1O)([O-:22])=[O:21]>>[CH3:17][N:13]1[C:12](=[O:18])[C:11]([NH:10][CH2:9][C:8]([N:5]2[CH2:4][CH2:3][CH:2]([O:1][C:24]3[CH:25]=[CH:26][CH:27]=[CH:28][C:23]=3[N+:20]([O-:22])=[O:21])[CH2:7][CH2:6]2)=[O:19])=[CH:16][CH:15]=[N:14]1

Participants

3

Reactant 2

HCID 69472-NitrophenolHCID 66957754HCID 66957754, compound

Product 1

HCID 66957741HCID 66957741, compoundYield 24%

Procedure

Compound 15 is prepared from intermediate 5b and from 2-nitro-phenol following synthesis method 3 (yield: 24%).

Sources & evidence

ORD record
ord-a649f35c5c9c40e8bb8578ae3a2a0db0
Source dataset
uspto-grants-2015_02
Patent number
US08946225B2

Reaction notes

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