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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1843254Generated: November 2, 2026

Hydrochloric Acid → HCID 86683764, compound

https://huagongshe.com/reaction/1843254

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86683763HCID 86683763—
SolventDiethyl EtherHCID 3283—
SolventDichloromethaneHCID 6344—
ProductHCID 86683764HCID 86683764120.7%

Reaction Steps

To the solution of 125c (1.19 g, 1.9 mmol) in dichloromethane (20 mL) was added 3M HCl in diethyl ether (15 mL). The reaction mixture was stirred at room temperature for 4 h. It was then concentrated under reduced pressure to afford 125d (900 mg, 95%). LCMS: [M+H]+ 392.1.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08946213B2
Source datasetuspto-grants-2015_02
ORD IDord-2d77f8c8ea2c4a28b3e4c2b29a012025
Source noteuspto-grants-2015_02