Ethanol → 4-[(2-Methoxypyridin-4-yl)oxy]-N2-methylbenzene-1,2-diamine

Participants

Reaction Steps

The reaction and post-treatment were carried out according to Example (1b) using 5-[(2-methoxypyridin-4-yl)oxy]-N-methyl-2-nitroaniline produced in Example (16c) (3.90 g, 14.2 mmol), iron powder (3.96 g, 70.8 mmol), ammonium chloride (0.38 g, 7.08 mmol), ethanol (80 mL) and water (40 mL) to obtain the title compound (3.46 g, 99%) as a brown oil.

Provenance & Evidence