Ethanol → HCID 86661630, compound

Participants

Reaction Steps

The reaction and post-treatment were carried out according to Example (1b) using tert-butyl{5-[(6-chloropyridin-3-yl)oxy]-2-nitrophenyl}methylcarbamate produced in Example (18a) (8.0 g, 21 mmol), iron powder (5.6 g, 105 mmol), ammonium chloride (0.56 g, 11 mmol), ethanol (40 mL) and water (20 mL) to obtain the title compound (7.4 g, 99%) as a brown oil.

Provenance & Evidence