HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 10039325, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 66803492 | HCID 66803492 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 10039325 | HCID 10039325 | 104.4% |
Reaction Steps
(Z)-1-(4-Methoxybenzyl)-3-(2-nitrovinyl)-1H-indole (5 g, 15.72 mmol) in dry THF (32 mL) was reacted with LAH (2.98 g, 78.61 mmol) in dry THF (32 mL). The resulting mixture was refluxed for 16 hours under nitrogen atmosphere to afford 4.6 g of the product (100% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946260B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-c6734ca149fb463db50183e2bcfa2cf9 |
| Source note | uspto-grants-2015_02 |