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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1843991Generated: November 3, 2026

Aluminium lithium hydride → HCID 10039325, compound

https://huagongshe.com/reaction/1843991

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAluminium lithium hydrideHCID 21226445—
ReactantHCID 66803492HCID 66803492—
SolventTetrahydrofuranHCID 8028—
ProductHCID 10039325HCID 10039325104.4%

Reaction Steps

(Z)-1-(4-Methoxybenzyl)-3-(2-nitrovinyl)-1H-indole (5 g, 15.72 mmol) in dry THF (32 mL) was reacted with LAH (2.98 g, 78.61 mmol) in dry THF (32 mL). The resulting mixture was refluxed for 16 hours under nitrogen atmosphere to afford 4.6 g of the product (100% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08946260B2
Source datasetuspto-grants-2015_02
ORD IDord-c6734ca149fb463db50183e2bcfa2cf9
Source noteuspto-grants-2015_02