4-methylnaphthalen-1-amine → HCID 59763695, compound

HRID 1844280Notes

Reaction equation

HRID 1844280 reaction equation
CC1C2C(=CC=CC=2)C(N)=CC=1.[CH2:13]([C:15]1[CH:24]=[CH:23][C:22]([N+:25]([O-])=O)=[C:21]2[C:16]=1[CH2:17][CH2:18][CH2:19][CH2:20]2)[CH3:14]>>[CH2:13]([C:15]1[C:16]2[CH2:17][CH2:18][CH2:19][CH2:20][C:21]=2[C:22]([NH2:25])=[CH:23][CH:24]=1)[CH3:14]

Participants

3

Reactant 2

HCID 4311874-methylnaphthalen-1-amineHCID 66632821HCID 66632821, compound

Product 1

HCID 59763695HCID 59763695, compound

Procedure

The procedure was essentially identical to the route for 4-Methyl-naphthalen-1-ylamine as described above, however, started with a solution of 5-ethyl-8-nitro-1,2,3,4-tetrahydro-naphthalene (795 mg, 3.95 mmol).

Sources & evidence

ORD record
ord-e843311c0b4e45e785725a5b5d35f39a
Source dataset
uspto-grants-2015_02
Patent number
US08946273B2

Reaction notes

Loading…