HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 136240906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 86727909 | HCID 86727909 | — |
| Product | HCID 136240906 | HCID 136240906 | 29% |
Reaction Steps
2-(Pyridine-3-ylethynyl)quinoline-5-ol (8.5 mg, 29%) was prepared as a yellow solid according to the same method as described in Example 16 except that 2-(pyridine-3-ylethynyl)quinoline-5-ylpivalate (40 mg, 0.121 mmol), LiAlH4 (0.3 mL, 1.0 M in THF), and THF (2.0 mL) were used.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946431B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-e3c4c5eb3c9842038dd79723e4e36f82 |
| Source note | uspto-grants-2015_02 |