HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenol → 3-(4-Chlorophenoxy)propan-1-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | 2,6-Dichlorophenol | HCID 6899 | — |
| Reactant | 3-(2,6-Dichlorophenoxy)propan-1-amine | HCID 3304286 | — |
| Product | 3-(4-Chlorophenoxy)propan-1-amine | HCID 6484654 | 85% |
Reaction Steps
Intermediate 11 (150 mg, 0.808 mmol, 85% yield) was prepared as a white powder following the procedure described for Intermediate 9 replacing 2,6-dichlorophenol with 4-chlorophenol as starting material. LC-MS (ESI) 186 (M+H), RT=1.41 min (Method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946430B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-b8e99765dcef43beb74ddbd54c20503d |
| Source note | uspto-grants-2015_02 |