(6-Bromo-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-diethyl-amine → N*2*,N*2*-Diethyl-[1,2,4]triazolo[1,5-a]pyridine-2,6-diamine

HRID 1844469Notes

Reaction equation

HRID 1844469 reaction equation
BrC1C=CC2N(N=C(N(CC)CC)N=2)C=1.[N:16]1([C:22]2[N:31]=[C:25]3[CH:26]=[CH:27][C:28]([NH2:30])=[CH:29][N:24]3[N:23]=2)[CH2:21][CH2:20]O[CH2:18][CH2:17]1>>[CH2:21]([N:16]([CH2:17][CH3:18])[C:22]1[N:31]=[C:25]2[CH:26]=[CH:27][C:28]([NH2:30])=[CH:29][N:24]2[N:23]=1)[CH3:20]

Participants

3

Reactant 2

HCID 89464394(6-Bromo-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-diethyl-amineHCID 894644042-Morpholin-4-yl-[1,2,4]triazolo[1,5-a]pyridin-6-amine

Product 1

HCID 89464363N*2*,N*2*-Diethyl-[1,2,4]triazolo[1,5-a]pyridine-2,6-diamine

Procedure

Using (6-bromo-[1,2,4]triazolo[1,5-a]pyridin-2-yl)-diethyl-amine, this compound was prepared following the same methods as for the synthesis of 2-morpholin-4-yl-[1,2,4]triazolo[1,5-a]pyridin-6-ylamine. Brown solid (500 mg, 66%). MS: m/z=206 (M+H+).

Workup

  1. customthis compound was prepared

Sources & evidence

ORD record
ord-41516bb5219a468b98f489214d822361
Source dataset
uspto-grants-2015_02
Patent number
US08946427B2

Reaction notes

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