Sodium Carbonate → HCID 70874058, compound

Participants

Reaction Steps

A solution of 1,3,5-tri-tert-butylbenzene (442 mg, 2.0 mmol) in ACN (20 mL) was cooled to 0° C. under N2. Selectfluor (1.06 g, 3.0 mmol) was added, keeping the temperature close to 0° C. The reaction was stirred overnight warming up to rt, poured into aq. Na2CO3 (15 mL) and extracted with Et2O (30 mL). The organic layer was washed with brine, dried with Na2SO4, filtered and evaporated to give compound P31a (430 mg, 81%).

Provenance & Evidence