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HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 1844787Erstellt: 25. Oktober 2026

Trimethylsilylacetylene → N-benzoyl-4-ethynyl-3-nitrobenzamide

https://huagongshe.com/reaction/1844787

Reaktionsgleichung

Beteiligte Stoffe

RolleNameHCIDEinwaage
EduktTrimethylsilylacetyleneHCID 66111—
EduktTrimethyl-2-propynylsilaneHCID 83378—
Edukt4-Iodo-3-nitrobenzoic acidHCID 11208598—
Edukt4-iodo-N-methyl-3-nitrobenzamideHCID 20755545—
ProduktN-benzoyl-4-ethynyl-3-nitrobenzamideHCID 57331455—

Reaktionsschritte

Compound I-14, Compound I-15, Compound I-16, Compound I-17, Compound I-18, Compound I-19, Compound I-20, Compound I-21, Compound I-22, Compound I-23, Compound I-24 and Compound I-25 were prepared sequentially according to the methods of Example 14, Example 15 and Example 16, by selecting appropriate amines and trimethylsilylacetylene, using the Compound 4-iodo-3-nitrobenzoic acid (Compound VI-1) as starting material; Compound I-26 was prepared sequentially according to the methods of Example 15 and Example 16, using the compound N-methyl-4-iodo-3-nitrobenzamide (Compound VII-1) and trimethylpropargylsilane as starting materials:

Herkunft & Nachweise

DOI10.6084/m9.figshare.5104873.v1
PatentnummerUS08946478B2
Quelldatensatzuspto-grants-2015_02
ORD IDord-5db980f8b4964d14b4ace38065301a1e
Quellennotizuspto-grants-2015_02