L-Aspartic Acid → HCID 86666372, compound

Participants

Reaction Conditions

Reaction Steps

82 mg L-aspartic acid was dissolved in 7 ml water at 70° C. A solution of 100 mg (0.58 mmol) rasagiline in 2 ml isopropanol was added at this temperature. The solution remained clear, was cooled to 0° C. and stirred at this temperature for 1 h. Since no turbidity was observed the solvents were removed in vacuo. The residual clear oil partially crystallised on standing. After a slurry wash with acetone, a white crystalline material was obtained (40 mg). Analysis revealed that this material was aspartic acid.

Provenance & Evidence