Hydrochloric Acid → HCID 86700930, compound

Participants

Reaction Steps

In a dried reaction flask, the crude (R)-butyl 3-(dimethylamino)pyrrolidine-1-carboxylate (2.0 g) obtained in the above step was added to CH2Cl2 (30 mL). HCl gas was passed thereto for 3 h. The solution was concentrated under reduced pressure to obtain a crude yellow viscous material (1.5 g).

Provenance & Evidence