HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 6,7-dimethoxy-3,4-dihydroisoquinoline-1-carboxylate → HCID 20202902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 6,7-dimethoxy-3,4-dihydroisoquinoline-1-carboxylate | HCID 4060727 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 20202902 | HCID 20202902 | 98% |
Reaction Steps
To a refluxing solution of 2.0 g (8.0 mmol) of 6,7-dimethoxy-3,4-dihydro-isoquinoline-1-carboxylic acid ethyl ester was added to 2.0 g of 10% Pd-C. After 12 h at reflux, the reaction mixture was cooled, filtered through celite, and evaporated under reduced pressure to provide 2.0 g (98%) of 6,7-dimethoxy-isoquinoline-1-carboxylic acid ethyl ester. LCMS: 262 (M+1)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08946259B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-32f758351eea42a1b253d1ed2111927b |
| Source note | uspto-grants-2015_02 |