Hydrochloric Acid → HCID 59824347, compound

Participants

Reaction Steps

Dioxane (52 ml), HCl (52 ml, 6 M) and 5 (6.5 g, 11 mmol) were mixed in a 250 ml round-bottom flask to form a pale slurry. The reaction mixture was heated to reflux for 30 minutes under argon. The now yellow solution was allowed to cool to room temperature and solvents were then removed on a rotary evaporator. The orange residue was then dissolved in 500 ml H2O and neutralized with a solution of NaHCO3 (sat.) under vigorous stirring. The precipitate formed was filtered off and washed several times with H2O giving a pale solid (4.7 g, 84%).

Provenance & Evidence