HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-nitrobenzoic acid → HCID 57859273, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-nitrobenzoic acid | HCID 7448 | — |
| Reactant | m-Aminoacetanilide | HCID 7604 | — |
| Product | HCID 57859273 | HCID 57859273 | — |
Reaction Steps
The compound S3 (Y═NH) was prepared using 2-chloro-4-nitrobenzoic acid and 3′-aminoacetanilide in the same way as S3 (Y═O). 1H-NMR (DMSO-d6) δ 11.54 (s, 1H), 8.32 (d, J=8.8, 1H), 8.26 (d, J=2.0, 1H), 7.92 (d, J=8.8, 1H), 7.86 (d, J=2.0, 8.4, 1H), 6.60 (dd, J=2.0, 8.8, 1H), 6.43 (d, J=2.0, 1H), 6.36 (bs, 2H). ESI-MS m/z (M+H) calc'd: 256.1, found 256.1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08951938B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-5b9b1e22d87f43599b5e921688066656 |
| Source note | uspto-grants-2015_02 |