HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-fluorobenzeneboronic acid → HCID 60168821, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-fluorobenzeneboronic acid | HCID 2773333 | — |
| Reactant | 5-Bromo-3-(1-(2,6-dichloro-3-fluorophenyl)ethoxy)pyridin-2-amine | HCID 21111478 | — |
| Reactant | methylphosphonoylmethane | HCID 178503022 | — |
| Product | HCID 60168821 | HCID 60168821 | — |
Reaction Steps
The title compound was prepared from 5-bromo-3-[1-(2,6-dichloro-3-fluoro-phenyl)-ethoxy]-pyridin-2-ylamine, 4-bromo-2-fluoro-phenyl boronic acid, and dimethylphosphine oxide following the same procedures as Example 1 Step 1 and Step 3; ESMS: m/z 471 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08951993B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-5f8f08905e4f4d328681da1044bd5c29 |
| Source note | uspto-grants-2015_02 |