HCID 66726708, compound → HCID 66727039, compound

HRID 1845960Notes

Reaction equation

HRID 1845960 reaction equation
Cl.Cl.NC1CCN(S(C2C=C3C(=CC=2)C=NC=C3)(=O)=O)CC1.[C:23]([O:27][C:28](N(CCCO)C[C@@H](NS(C1C=C2C(=CC=1)C=NC=C2)(=O)=O)C)=[O:29])([CH3:26])([CH3:25])[CH3:24].Cl.Cl.[Br:54][C:55]1[C:64]([S:65]([N:68]2[CH2:75][CH2:74][CH2:73][CH2:72][NH:71][CH2:70][C@H:69]2[CH3:76])(=[O:67])=[O:66])=[CH:63][CH:62]=[C:61]2[C:56]=1[CH:57]=[CH:58][N:59]=[CH:60]2>>[Br:54][C:55]1[C:64]([S:65]([N:68]2[CH2:75][CH2:74][CH2:73][CH2:72][N:71]([C:28]([O:27][C:23]([CH3:26])([CH3:25])[CH3:24])=[O:29])[CH2:70][C@H:69]2[CH3:76])(=[O:67])=[O:66])=[CH:63][CH:62]=[C:61]2[C:56]=1[CH:57]=[CH:58][N:59]=[CH:60]2

Participants

4

Reactant 3

HCID 66726708HCID 66726708, compoundHCID 66727128HCID 66727128, compoundHCID 66727253HCID 66727253, compound

Product 1

HCID 66727039HCID 66727039, compound

Procedure

The compound of interest was synthesized (colorless oil, 41%) according to the production method of Step 1 of Example 12 using Reference Compound 4 instead of Reference Compound 2 and using Reference Compound 23 instead of Reference Compound 9.

Workup

  1. customThe compound of interest was synthesized (colorless oil, 41%)

Sources & evidence

ORD record
ord-725a21a411884d738951c9a1ff79e792
Source dataset
uspto-grants-2015_02
Patent number
US08951997B2

Reaction notes

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