HCID 43377434, compound → HCID 43510731, compound

Participants

Reaction Steps

A mixture of N-(4-Bromophenyl)-2-fluoro-5-nitro-benzoic acid amide (1.57 g, 4.6 mmol) and 500 mg Ra-Ni in 100 mL THF was stirred for 20 h under an atmosphere of hydrogen (3 bar). After filtration and concentration i. vac. the subtitle compound was obtained. Yield: 1.46 g (quantitative). MS [M+H]+=309 (Br-isotope pattern); TLC: Rf=0.68 (silica gel, DCM:EtOH 9:1).

Provenance & Evidence