HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-4,6-dinitrophenol → 2,4-Diamino-6-methylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-4,6-dinitrophenol | HCID 10800 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2,4-Diamino-6-methylphenol | HCID 27520 | — |
Reaction Steps
11.0 g (50.0 mmol) 4,6-dinitro-o-cresol were hydrogenated with 2.0 g Raney nickel in 100 mL MeOH under a 5 bar hydrogen atmosphere for 4 h at RT. Then the catalyst was suction filtered and the filtrate was concentrated by rotary evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08952014B2 |
| Source dataset | uspto-grants-2015_02 |
| ORD ID | ord-5bf0471307164afaa7fad54b9211d700 |
| Source note | uspto-grants-2015_02 |